4-Chloro-2-fluorobenzonitrile → [3-(5-Chloro-2-cyanophenoxy)pentyl]methylcarbamic acid, 1,1-dimethylethyl ester

HRID 2183839Notes

Reaction equation

HRID 2183839 reaction equation
[OH:1][CH:2]([CH2:14][CH3:15])[CH2:3][CH2:4][N:5]([CH3:13])[C:6](=[O:12])[O:7][C:8]([CH3:11])([CH3:10])[CH3:9].[Cl:16][C:17]1[CH:24]=[CH:23][C:20]([C:21]#[N:22])=[C:19](F)[CH:18]=1>>[Cl:16][C:17]1[CH:18]=[CH:19][C:20]([C:21]#[N:22])=[C:23]([CH:24]=1)[O:1][CH:2]([CH2:14][CH3:15])[CH2:3][CH2:4][N:5]([CH3:13])[C:6](=[O:12])[O:7][C:8]([CH3:10])([CH3:11])[CH3:9]

Participants

3

Reactant 2

HCID 936554-Chloro-2-fluorobenzonitrileHCID 857904251,1-Dimethylethyl (3-hydroxypentyl)methylcarbamate

Product 1

HCID 90837505[3-(5-Chloro-2-cyanophenoxy)pentyl]methylcarbamic acid, 1,1-dimethylethyl ester

Procedure

The title compound was prepared according to the method of Example 3 step (b) but using (3-hydroxypentyl)methylcarbamic acid, 1,1-dimethylethyl ester and 4-chloro-2-fluorobenzonitrile.

Sources & evidence

ORD record
ord-ac6a0ebfb43741f08ae243912c5f8d6a
Source dataset
uspto-grants-2005_05
Patent number
US06900243B2

Reaction notes

Loading…