4-Chloro-2-fluoro-1-nitrobenzene → [3-(5-Chloro-2-nitrophenoxy)pentyl]methylcarbamic acid, 1,1-dimethylethyl ester

HRID 2183844Notes

Reaction equation

HRID 2183844 reaction equation
[OH:1][CH:2]([CH2:14][CH3:15])[CH2:3][CH2:4][N:5]([CH3:13])[C:6](=[O:12])[O:7][C:8]([CH3:11])([CH3:10])[CH3:9].[Cl:16][C:17]1[CH:22]=[CH:21][C:20]([N+:23]([O-:25])=[O:24])=[C:19](F)[CH:18]=1>>[Cl:16][C:17]1[CH:18]=[CH:19][C:20]([N+:23]([O-:25])=[O:24])=[C:21]([CH:22]=1)[O:1][CH:2]([CH2:14][CH3:15])[CH2:3][CH2:4][N:5]([CH3:13])[C:6](=[O:12])[O:7][C:8]([CH3:10])([CH3:11])[CH3:9]

Participants

3

Reactant 2

HCID 696914-Chloro-2-fluoro-1-nitrobenzeneHCID 857904251,1-Dimethylethyl (3-hydroxypentyl)methylcarbamate

Product 1

HCID 91106314[3-(5-Chloro-2-nitrophenoxy)pentyl]methylcarbamic acid, 1,1-dimethylethyl ester

Procedure

The title compound was prepared according to the method of Example 3 step (b) but using (3-hydroxypentyl)methylcarbamic acid, 1,1-dimethylethyl ester and 4-chloro-2-fluoronitrobenzene.

Sources & evidence

ORD record
ord-1ee1c5bc6a4146edaa2cf58b1337bfc3
Source dataset
uspto-grants-2005_05
Patent number
US06900243B2

Reaction notes

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