HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzonitrile, 4-bromo- → HCID 22285304, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzonitrile, 4-bromo- | HCID 12162 | — |
| Reactant | 2-Fluoro-5-nitrophenylboronic acid, pinacol ester | HCID 3833297 | — |
| Product | HCID 22285304 | HCID 22285304 | — |
Reaction Steps
4-Bromobenzonitrile and 2-(2-fluoro-5-nitrophenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane were coupled using the procedure described in Example 1 to afford 2′-fluoro-5′-nitrobiphenyl-4-carbonitrile as a brown solid: δH (400 MHz, CDCl3) 7.37 (1H, dd, J 9 and 9), 7.70 (2H, dd, J 8 and 1), 7.80 (1H, dd, J 8 and 1), 8.29-8.33 (1H, m), 8.37-8.40 (1H, m).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06900215B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-79fa5924e5fa413896f48f2f4556145b |
| Source note | uspto-grants-2005_05 |