HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-6-nitrotoluene → HCID 22473548, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-6-nitrotoluene | HCID 123537 | — |
| Reactant | 5-Fluoro-2-(tetramethyl-1,3,2-dioxaborolan-2-yl)benzonitrile | HCID 22180790 | — |
| Product | HCID 22473548 | HCID 22473548 | — |
Reaction Steps
2-Bromo-6-nitrotoluene and 5-fluoro-2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)benzonitrile were coupled using the procedure described in Example 1 to afford crude 4-fluoro-2′-methyl-3′-nitrobiphenyl-2-carbonitrile as a black solid: δH (360 MHz, CDCl3) 2.32 (3H, s), 7.34-7.46 (5H, m), 7.95 (1H, m).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06900215B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-69a04841e22347f2bc238744a70bf68e |
| Source note | uspto-grants-2005_05 |