HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bis(neopentyl glycolato)diboron → 4-Fluoro-3-([1,2,4]triazol-1-yl)phenylboronic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bis(neopentyl glycolato)diboron | HCID 2734316 | — |
| Reactant | 1-(5-Bromo-2-fluorophenyl)-1h-[1,2,4]triazole | HCID 22329542 | — |
| Product | 4-Fluoro-3-([1,2,4]triazol-1-yl)phenylboronic acid | HCID 22329489 | — |
Reaction Steps
1-(5-Bromo-2-fluorophenyl)-1H-[1,2,4]triazole (1.1 g, 4.5 mmol) was reacted with bis(neopentyl glycolato)diboron (1.13 g, 5.0 mmol) using the method in Example 51 to give 4-fluoro-3-([1,2,4]triazol-1-yl)phenylboronic acid as a white solid: m/z (ES+) 208 (M++H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06900215B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-7b0929c96f7f4adc8225a8b8709a07e4 |
| Source note | uspto-grants-2005_05 |