HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperazine, 4-benzoyl-1-(1,2-dioxo-2-(1H-pyrrolo(2,3-b)pyridin-3-yl)ethyl)-2-methyl-, (2R)- → n-(Benzoyl)-3-methyl-n'-[(4,7-dimethoxy-6-azaindol-3-yl)-oxoacetyl]piperazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperazine, 4-benzoyl-1-(1,2-dioxo-2-(1H-pyrrolo(2,3-b)pyridin-3-yl)ethyl)-2-methyl-, (2R)- | HCID 5495793 | — |
| Reactant | Potassium (4,7-dimethoxy-6-azaindol-3-yl)-oxoacetate | HCID 22893810 | — |
| Product | n-(Benzoyl)-3-methyl-n'-[(4,7-dimethoxy-6-azaindol-3-yl)-oxoacetyl]piperazine | HCID 22476268 | — |
Reaction Steps
Compound 5ap, ®-N-(benzoyl)-3-methyl-N′-[(4,7-dimethoxy-6-azaindol-3-yl)-oxoacetyl]-piperazine (white solid) was prepared using the same method used to prepare compound 5a except that Potassium (4,7-dimethoxy-6-azaindol-3-yl)-oxoacetate was used as the starting material. MS m/z: (M+H)+ calcd for C23H25N4O5: 437.18; found 437.24. HPLC retention time: 1.37 minutes (column B).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06900323B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-9be079a7f829472496710911baf12bbe |
| Source note | uspto-grants-2005_05 |