HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tri(2-ethylhexyl)amine → 5-Butoxy-4-methyl-1,3-oxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tri(2-ethylhexyl)amine | HCID 102705 | — |
| Reactant | n-Butyl alpha-isocyanopropionate | HCID 11171108 | — |
| Solvent | Chlorobenzene | HCID 7964 | — |
| Product | 5-Butoxy-4-methyl-1,3-oxazole | HCID 9877440 | — |
Reaction Steps
A column according to example 1 but without a dividing wall (see FIG. 1) was continuously charged via inlet (A) with a mixture of 20.6% by weight of chlorobenzene, 5.2% by weight of n-butyl α-isocyanopropionate (R1=n-butyl, R2=methyl) and 72.60% by weight of tris(2-ethylhexyl)amine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06900332B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-312a9549597e4547b328fa5943b4196a |
| Source note | uspto-grants-2005_05 |