Tri(2-ethylhexyl)amine → 5-Butoxy-4-methyl-1,3-oxazole

HRID 2184281Notes

Reaction equation

HRID 2184281 reaction equation
[N+:1]([CH:3]([CH3:11])[C:4]([O:6][CH2:7][CH2:8][CH2:9][CH3:10])=[O:5])#[C-:2].C(C(CCCC)CN(CC(CC)CCCC)CC(CC)CCCC)C>>[CH3:11][C:3]1[N:1]=[CH:2][O:5][C:4]=1[O:6][CH2:7][CH2:8][CH2:9][CH3:10]

Participants

3

Reactant 2

HCID 102705Tri(2-ethylhexyl)amineHCID 11171108n-Butyl alpha-isocyanopropionate

Product 1

HCID 98774405-Butoxy-4-methyl-1,3-oxazole

Procedure

Example 3 was repeated, except that a mixture of 13.14% by weight of n-butyl α-isocyanopropionate and 86.86% by weight of tris(2-ethylhexyl)amine was continuously added via inlet (A).

Sources & evidence

ORD record
ord-2ec0c49429e04311b3584eca01d201e7
Source dataset
uspto-grants-2005_05
Patent number
US06900332B2

Reaction notes

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