HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boc-D-Tyr(Me)-L-Ile-D-Pro-OBzl → Boc-D-Tyr(Me)-L-Ile-D-Pro-OH
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boc-D-Tyr(Me)-L-Ile-D-Pro-OBzl | HCID 58726683 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Boc-D-Tyr(Me)-L-Ile-D-Pro-OH | HCID 131723245 | — |
Reaction Steps
The compound Boc-D-Tyr(Me)-L-Ile-D-Pro-OBzl (881 mg, 1.44 mmol) obtained in step 12-4 was dissolved in MeOH (5 ml) and stirred under hydrogen atmosphere overnight using 5% Pd/C (70 mg). The reaction mixture was filtered and concentrated to yield the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06399568B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-3bac5502f3ed4c97a94eb197bd64ca64 |
| Source note | uspto-grants-2002_06 |