HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → HCID 18399709, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 18399751 | HCID 18399751 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 18399709 | HCID 18399709 | — |
Reaction Steps
1 g of the product obtained in Step E is added dropwise to a suspension of 93 ml of ethyl chloroformate and 0.89 g of K2CO3 in 5 ml of toluene. After 12 hours at ambient temperature, the reaction mixture is diluted with water, extracted with toluene and then concentrated under reduced pressure. Chromatography on silica gel (dichloromethane/methanol: 95/5) enables the expected product to be isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06399616B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-e4d17f8d3c184c709aa7c16f821b0bbc |
| Source note | uspto-grants-2002_06 |