Hydroquinone → HCID 22458102, compound

Participants

Reaction Conditions

Reaction Steps

A suspension of compound 85B (0.106 g), hydroquinone (0.003 g) in 2 N HCl (1.14 mL) was heated at 80° C. for 30-40 minutes. After cooling to room temperature, NaHCO3 was added (pH=7) and the resulting mixture was extracted with CH2Cl2 (3×10 mL).The combined organic layers were dried (Na2SO4), filtered and evaporated to dryness at reduced pressure to give 0.081 g (88%) of the title compound as an oil.

Provenance & Evidence