HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dichloroaniline → Ethyl N-(3,4-dichlorophenyl)alaninate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dichloroaniline | HCID 7257 | — |
| Reactant | Ethyl pyruvate | HCID 12041 | — |
| Product | Ethyl N-(3,4-dichlorophenyl)alaninate | HCID 169545 | — |
Reaction Steps
Following General Procedure A above and using 3,4-dichloroaniline (Aldrich) and ethyl pyruvate (Aldrich), the title compound was prepared as an oil. The reaction was monitored by tlc on silica gel (Rf=0.4 in 25% EtOAc/hexanes) and purification was by preparative plate chromatography (silica gel using 25 % EtOAc/hexanes as the eluant).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06399628B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-af29860bbbcf43c684cc01421ee7f404 |
| Source note | uspto-grants-2002_06 |