HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl Alcohol → N-(3,4dichlorophenyl)alanine Allyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl Alcohol | HCID 7858 | — |
| Reactant | N-(3,4-dichlorophenyl)alanine Methyl Ester | HCID 54289412 | — |
| Product | N-(3,4dichlorophenyl)alanine Allyl Ester | HCID 53861976 | — |
Reaction Steps
Following transesterification General Procedure B above and using N-(3,4-dichlorophenyl)alanine methyl ester (from Example 9 above) and allyl alcohol (Aldrich), the title compound was prepared as an oil. The reaction was monitored by silica gel tlc (Rf=0.62 in 25% EtOAc/hexanes). Purification was by preparative plate chromatography (silica gel using 25% EtOAc/hexanes as the eluant).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06399628B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-14ee4fca54214576b091cc22b05fc48a |
| Source note | uspto-grants-2002_06 |