9H-xanthene-9-carbonyl chloride → HCID 9923127, compound
Reaction equation
[NH2:1][C:2]1[N:3]=[N:4][N:5]([CH2:7][CH3:8])[N:6]=1.[CH:9]1[C:22]2[CH:21]([C:23](Cl)=[O:24])[C:20]3[C:15](=[CH:16][CH:17]=[CH:18][CH:19]=3)[O:14][C:13]=2[CH:12]=[CH:11][CH:10]=1>>[CH2:7]([N:5]1[N:4]=[N:3][C:2]([NH:1][C:23]([CH:21]2[C:22]3[CH:9]=[CH:10][CH:11]=[CH:12][C:13]=3[O:14][C:15]3[C:20]2=[CH:19][CH:18]=[CH:17][CH:16]=3)=[O:24])=[N:6]1)[CH3:8]Participants
3
Procedure
The title compound, white solid, m.p. 228° C. (dec.) and MS: (neg. ions): m/e=320.0 (M+−H) was prepared in accordance with the general method of example 1 from 5-amino-2-ethyl-2H-tetrazole and 9H-xanthene-9-carbonyl chloride.
Sources & evidence
- ORD record
- ord-fc480dce406845d99f086bfdfadfa95d
- Source dataset
- uspto-grants-2002_06
- Patent number
- US06399641B1
Reaction notes
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