9H-xanthene-9-carbonyl chloride → HCID 9880661, compound

HRID 2184981Notes

Reaction equation

HRID 2184981 reaction equation
[NH2:1][C:2]1[N:3]=[N:4][N:5]([CH2:7][C:8]#[N:9])[N:6]=1.[CH:10]1[C:23]2[CH:22]([C:24](Cl)=[O:25])[C:21]3[C:16](=[CH:17][CH:18]=[CH:19][CH:20]=3)[O:15][C:14]=2[CH:13]=[CH:12][CH:11]=1>>[C:8]([CH2:7][N:5]1[N:4]=[N:3][C:2]([NH:1][C:24]([CH:22]2[C:23]3[CH:10]=[CH:11][CH:12]=[CH:13][C:14]=3[O:15][C:16]3[C:21]2=[CH:20][CH:19]=[CH:18][CH:17]=3)=[O:25])=[N:6]1)#[N:9]

Participants

3

Procedure

The title compound, white solid, m.p. 204-205° and MS: m/e=333.2 (M++H) was prepared in accordance with the general method of example 1 from (5-amino-tetrazol-2-yl)-acetonitrile and 9H-xanthene-9-carbonyl chloride.

Sources & evidence

ORD record
ord-806e81ee81834fa5be26006f79d515b5
Source dataset
uspto-grants-2002_06
Patent number
US06399641B1

Reaction notes

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