2-ethyl-2H-tetrazol-5-amine → HCID 9858931, compound

HRID 2184985Notes

Reaction equation

HRID 2184985 reaction equation
[NH2:1][C:2]1[N:3]=[N:4][N:5]([CH2:7][CH3:8])[N:6]=1.[CH:9]1[C:19]2[CH:18]([C:20](Cl)=[O:21])[C:17]3[CH:23]=[CH:24][CH:25]=[CH:26][C:16]=3[CH2:15][O:14][C:13]=2[CH:12]=[CH:11][CH:10]=1>>[CH2:7]([N:5]1[N:4]=[N:3][C:2]([NH:1][C:20]([CH:18]2[C:17]3[CH:23]=[CH:24][CH:25]=[CH:26][C:16]=3[CH2:15][O:14][C:13]3[CH:12]=[CH:11][CH:10]=[CH:9][C:19]2=3)=[O:21])=[N:6]1)[CH3:8]

Participants

3

Reactant 2

HCID 42745882-ethyl-2H-tetrazol-5-amineHCID 22459195HCID 22459195, compound

Product 1

HCID 9858931HCID 9858931, compound

Procedure

The title compound, yellow solid, m.p. 158-159° and MS: (neg. ions): m/e=334.1 (M+−H) was prepared in accordance with the general method of example 1 from 5-amino-2-ethyl-2H-tetrazole and 6,11 -dihydro-dibenzo[b,e]oxepine-11-carbonyl chloride.

Sources & evidence

ORD record
ord-f0caf63213f24c36a7044852cad38e90
Source dataset
uspto-grants-2002_06
Patent number
US06399641B1

Reaction notes

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