2-ethyl-2H-tetrazol-5-amine → HCID 9968318, compound
Reaction equation
[NH2:1][C:2]1[N:3]=[N:4][N:5]([CH2:7][CH3:8])[N:6]=1.[CH3:9][O:10][C:11]1[C:24]2[CH:23]([C:25](Cl)=[O:26])[C:22]3[C:17](=[CH:18][CH:19]=[CH:20][CH:21]=3)[O:16][C:15]=2[CH:14]=[CH:13][CH:12]=1>>[CH2:7]([N:5]1[N:4]=[N:3][C:2]([NH:1][C:25]([CH:23]2[C:24]3[C:11]([O:10][CH3:9])=[CH:12][CH:13]=[CH:14][C:15]=3[O:16][C:17]3[C:22]2=[CH:21][CH:20]=[CH:19][CH:18]=3)=[O:26])=[N:6]1)[CH3:8]Participants
3
Procedure
The title compound, white solid, m.p. 259-260° C. (dec.) and MS: (pos. ions): m/e=352.3 (M++H) was prepared in accordance with the general method of example 1 from 5-amino-2-ethyl-2H-tetrazole and (RS)-1-methoxy-9H-xanthene-9-carbonyl chloride.
Sources & evidence
- ORD record
- ord-a5a2bcd2e28c41eebf9fdb6d449dec23
- Source dataset
- uspto-grants-2002_06
- Patent number
- US06399641B1
Reaction notes
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