2-ethyl-2H-tetrazol-5-amine → HCID 10132627, compound
Reaction equation
[NH2:1][C:2]1[N:3]=[N:4][N:5]([CH2:7][CH3:8])[N:6]=1.[CH3:9][O:10][C:11]1[C:24]2[O:23][C:22]3[C:17](=[CH:18][CH:19]=[CH:20][CH:21]=3)[CH:16]([C:25](Cl)=[O:26])[C:15]=2[CH:14]=[CH:13][CH:12]=1>>[CH2:7]([N:5]1[N:4]=[N:3][C:2]([NH:1][C:25]([CH:16]2[C:15]3[CH:14]=[CH:13][CH:12]=[C:11]([O:10][CH3:9])[C:24]=3[O:23][C:22]3[C:17]2=[CH:18][CH:19]=[CH:20][CH:21]=3)=[O:26])=[N:6]1)[CH3:8]Participants
3
Procedure
The title compound, white solid, m.p. 239-240° C. (dec.) and MS: (pos. ions): m/e=352.3 (M++H) was prepared in accordance with the general method of example 1 from 5-amino-2-ethyl-2H-tetrazole and (RS)-4-methoxy-9H-xanthene-9-carbonyl chloride.
Sources & evidence
- ORD record
- ord-e76cf77d228b45238a6b21359e0f447b
- Source dataset
- uspto-grants-2002_06
- Patent number
- US06399641B1
Reaction notes
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