Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Iodo-3-methylaniline → 3-Allyl-1-(4-amino-2-methylphenyl)piperidin-2-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Iodo-3-methylaniline | HCID 2734275 | — |
| 반응물 | 3-Allyl-2-piperidinone | HCID 13380374 | — |
| 생성물 | 3-Allyl-1-(4-amino-2-methylphenyl)piperidin-2-one | HCID 59586720 | — |
반응 단계
Analogously to the process described under example 93A, 2.68 g (11.5 mmol) of 4-iodo-3-methylaniline and 2.0 g (14.3 mmol) of the compound from example 96A are used to obtain, after preparative HPLC, 1.31 g (47% of theory) of the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08198267B2 |
| 출처 데이터셋 | uspto-grants-2012_06 |
| ORD ID | ord-e6f96413f81047488b5322cb44ec1148 |
| 출처 메모 | uspto-grants-2012_06 |