HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 16248099, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 1,1'-Biphenyl, 4-(bromomethyl)- | HCID 257716 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 16248099 | HCID 16248099 | 90.5% |
Reaction Steps
Triphenylphosphine (1.34 g) was added to a stirred solution of 4-phenylbenzyl bromide (1.26 g) in xylene (20 mL). The mixture was refluxed for 19 hr to a give white solid. The solid was washed with toluene and hexane to afford the titled compound (2.35 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06399629B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-0fcab3112afa4c3986fa712323309a7a |
| Source note | uspto-grants-2002_06 |