Sodium Iodide → HCID 21341522, compound

Participants

Reaction Conditions

Reaction Steps

The product from (B) (12.6 mmol) was dissolved in DMF (25 mL) and sodium azide (NaN3) (50 mmol) and sodium iodide (NaI) (50 mmol) were added. This solution was warmed at 50° C. for 24 hr then cooled to room temperature, washed with H2O (3×50 mL), extracted with EtOAc (2×50 mL) and washed with brine (1×25 mL). The organic layer was dried over Na2SO4, filtered dried to give the title compound (2.8 g, 77%) as an oil.

Provenance & Evidence