反应详情

N-(2-Phenylethyl)-2-nitroaniline (3.0 g, 12.4 mmol) was dissolved in MeOH (60 mL), and 10% Pd/C (300mg) was added. The mixture was hydrogenated at 1 atm for 18 hrs at room temperature, filtered over a celite pad and concentrated to an oil. The resulting oil was applied to a column prepacked with silica. The title compound was eluted from the column with EtOAc/Hexanes (1:3, v:v).

1. filtrationfiltered over a celite pad
2. concentrationconcentrated to an oil
3. washThe title compound was eluted from the column with EtOAc/Hexanes (1:3, v:v)