HuagongsheHuagongshe Chemistry Print Report · For research reference only
[(4-Dimethylaminophenyl)methyl](4-ethylphenyl)amine → N-[(4-dimethylaminophenyl)methyl]-N-(4-ethylphenyl)-6,7,8,9-tetrahydro-5H-benzocycloheptene-5-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | [(4-Dimethylaminophenyl)methyl](4-ethylphenyl)amine | HCID 3482181 | — |
| Reactant | 6,7,8,9-tetrahydro-5H-benzo(7)annulene-5-carboxylic acid | HCID 14822604 | — |
| Product | N-[(4-dimethylaminophenyl)methyl]-N-(4-ethylphenyl)-6,7,8,9-tetrahydro-5H-benzocycloheptene-5-carboxamide | HCID 10202735 | 19.9% |
Reaction Steps
By the reaction and treatment in the same manner as in Example 1 using 6,7,8,9-tetrahydro-5H-benzocycloheptene-5-carboxylic acid (0.54 g) and [(4-dimethylaminophenyl)methyl](4-ethylphenyl)amine (0.6 g) as starting materials, N-[(4-dimethylaminophenyl)methyl]-N-(4-ethylphenyl)-6,7,8,9-tetrahydro-5H-benzocycloheptene-5-carboxamide (0.2 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08198454B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-e97a9f9b53c841b6a3c763bd7ce59487 |
| Source note | uspto-grants-2012_06 |