HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,6-Hexanediol → HCID 20663734, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,6-Hexanediol | HCID 12374 | — |
| Reactant | 2,2-Dimethyl-1,3-dioxane-4,6-dione | HCID 16249 | — |
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Product | HCID 20663734 | HCID 20663734 | — |
Reaction Steps
A solution of bis-(6-hydroxyhexyl) malonate in 1,6-hexanediol is prepared by heating a mixture of 21.6 g (0.15 mol) of Meldrum's acid, 59 g (0.50 mol) of 1,6-hexanediol and 0.28 g (1.5 mmol) of p-toluene-sulphonic acid monohydrate for 2 hours at 140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06403239B2 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-89c7519f8796446e93c1d8de4947952f |
| Source note | uspto-grants-2002_06 |