HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dihydro-2H-1-benzothiopyran-4-carboxylic acid → HCID 10203919, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dihydro-2H-1-benzothiopyran-4-carboxylic acid | HCID 188668 | — |
| Reactant | N-(4-(Dimethylamino)benzyl)-4-isopropylbenzenamine | HCID 21957887 | — |
| Product | HCID 10203919 | HCID 10203919 | 28.7% |
Reaction Steps
By the reaction and treatment in the same manner as in Example 1 using thiochroman-4-carboxylic acid (0.55 g) and [(4-dimethylaminophenyl)methyl](4-isopropylphenyl)amine (0.63 g) as starting materials, N-[(4-dimethylaminophenyl)methyl]-N-(4-isopropylphenyl)thiochroman-4-carboxamide (0.3 g) was obtained. melting point: 118° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08198454B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-e46f592e553641499b031f7e31e13569 |
| Source note | uspto-grants-2012_06 |