1-Bromo-2-methylpropane → HCID 22452245, compound

HRID 2185787Notes

Reaction equation

HRID 2185787 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([C:10]2[CH:11]=[C:12]([C:17]([O:19][CH3:20])=[O:18])[C:13](=[O:16])[NH:14][N:15]=2)[CH:5]=[CH:6][C:7]=1[O:8][CH3:9].Br[CH2:22][CH:23]([CH3:25])[CH3:24]>>[Cl:1][C:2]1[CH:3]=[C:4]([C:10]2[CH:11]=[C:12]([C:17]([O:19][CH3:20])=[O:18])[C:13](=[O:16])[N:14]([CH2:22][CH:23]([CH3:25])[CH3:24])[N:15]=2)[CH:5]=[CH:6][C:7]=1[O:8][CH3:9]

Participants

3

Reactant 2

HCID 65551-Bromo-2-methylpropaneHCID 22452271HCID 22452271, compound

Product 1

HCID 22452245HCID 22452245, compoundYield 79.5%

Procedure

Using 6-(3-chloro-4-methoxyphenyl)-4-methoxycarbonyl-2H-pyridazin-3-one and 1-bromo-2-methylpropane as starting materials, the procedures of Example 1 were repeated likewise, whereby the title compound was obtained in a yield of 79.5%.

Sources & evidence

ORD record
ord-b826f7fe1a174cb6b2bf50ead6fd2bff
Source dataset
uspto-grants-2002_06
Patent number
US06403586B1

Reaction notes

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