1-Bromo-2-methylpropane → 2-Isobutyl-4-methoxycarbonyl-6-[4-(methylthio)phenyl]-2H-pyridazin-3-one
반응식
[CH3:1][O:2][C:3]([C:5]1[C:6](=[O:19])[NH:7][N:8]=[C:9]([C:11]2[CH:16]=[CH:15][C:14]([S:17][CH3:18])=[CH:13][CH:12]=2)[CH:10]=1)=[O:4].Br[CH2:21][CH:22]([CH3:24])[CH3:23]>>[CH2:21]([N:7]1[C:6](=[O:19])[C:5]([C:3]([O:2][CH3:1])=[O:4])=[CH:10][C:9]([C:11]2[CH:16]=[CH:15][C:14]([S:17][CH3:18])=[CH:13][CH:12]=2)=[N:8]1)[CH:22]([CH3:24])[CH3:23]참가 물질
3
실험 절차
Using 4-methoxycarbonyl-6-[4-(methylthio)phenyl]-2H-pyridazin-3-one and 1-bromo-2-methylpropane as starting materials, the procedures of Example 1 were repeated likewise, whereby the title compound was obtained in a yield of 77.3%.
출처 및 근거
- ORD 기록
- ord-cbcc4155356e44959182a703239d1fb3
- 출처 데이터셋
- uspto-grants-2002_06
- 특허 번호
- US06403586B1
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