2-Butene, 1-bromo-3-methyl- → HCID 12971768, compound

HRID 2185789Notes

Reaction equation

HRID 2185789 reaction equation
[CH2:1]([O:3][C:4]([C:6]1[C:7](=[O:20])[NH:8][N:9]=[C:10]([C:12]2[CH:17]=[CH:16][C:15]([O:18][CH3:19])=[CH:14][CH:13]=2)[CH:11]=1)=[O:5])[CH3:2].Br[CH2:22][CH:23]=[C:24]([CH3:26])[CH3:25]>>[CH2:1]([O:3][C:4]([C:6]1[C:7](=[O:20])[N:8]([CH2:22][CH:23]=[C:24]([CH3:26])[CH3:25])[N:9]=[C:10]([C:12]2[CH:13]=[CH:14][C:15]([O:18][CH3:19])=[CH:16][CH:17]=2)[CH:11]=1)=[O:5])[CH3:2]

Participants

3

Reactant 2

HCID 700922-Butene, 1-bromo-3-methyl-HCID 22452278HCID 22452278, compound

Product 1

HCID 12971768HCID 12971768, compoundYield 87.6%

Procedure

Using 4-ethoxycarbonyl-6-(4-methoxyphenyl)-2H-pyridazin-3-one and 1-bromo-3-methyl-2-butene as starting materials, the procedures of Example 1 were repeated likewise, whereby the title compound was obtained in a yield of 87.6%.

Sources & evidence

ORD record
ord-cdeb684f48644e20b47e05584bd61d80
Source dataset
uspto-grants-2002_06
Patent number
US06403586B1

Reaction notes

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