HCID 15453537, compound → HCID 22452227, compound

HRID 2185808Notes

Reaction equation

HRID 2185808 reaction equation
[CH3:1][O:2][C:3]([C:5]1[C:6](=[O:19])[NH:7][N:8]=[C:9]([C:11]2[CH:16]=[CH:15][C:14]([O:17][CH3:18])=[CH:13][CH:12]=2)[CH:10]=1)=[O:4].Br[CH2:21][C:22]([NH:24][C:25]1[CH:30]=[CH:29][C:28]([S:31][CH3:32])=[CH:27][CH:26]=1)=[O:23]>>[CH3:1][O:2][C:3]([C:5]1[C:6](=[O:19])[N:7]([CH2:21][C:22](=[O:23])[NH:24][C:25]2[CH:30]=[CH:29][C:28]([S:31][CH3:32])=[CH:27][CH:26]=2)[N:8]=[C:9]([C:11]2[CH:16]=[CH:15][C:14]([O:17][CH3:18])=[CH:13][CH:12]=2)[CH:10]=1)=[O:4]

Participants

3

Reactant 2

HCID 15453537HCID 15453537, compoundHCID 22452250HCID 22452250, compound

Product 1

HCID 22452227HCID 22452227, compoundYield 90%

Procedure

Using 4-methoxycarbonyl-6-(4-methoxyphenyl)-2H-pyridazin-3-one and 2-bromo-4′-(methylthio)acetanilide as starting materials, the procedures of Example 1 were repeated likewise, whereby the title compound was obtained in a yield of 90.0%.

Sources & evidence

ORD record
ord-39db49f8e5274baa99c732d619701c90
Source dataset
uspto-grants-2002_06
Patent number
US06403586B1

Reaction notes

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