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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2186280Generated: November 1, 2026

HCID 86586189, compound → HCID 86586190, compound

https://huagongshe.com/reaction/2186280

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86586189HCID 86586189—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 86586190HCID 8658619070%

Reaction Steps

0.80 g of 6-t-butyl-5-hydroxy-4-(2-methyl-2-propenyl)-2,3-dihydrobenzofuran-2-spiro-1′-cycloheptane synthesized in Example 10 was dissolved in 5 ml of ethanol and the solution was treated with 0.05 g of 10% palladium on carbon in the same manner as in Example 9 to give 0.56 g of 6-t-butyl-5-hydroxy-4-(2-methylpropyl)-2,3-dihydrobenzofuran-2-spiro-1′-cycloheptane as a pale yellow oil (yield 70%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06403639B1
Source datasetuspto-grants-2002_06
ORD IDord-9c2190eba1b546e0b628aa7a699f5d77
Source noteuspto-grants-2002_06