HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69890713, compound → HCID 86586191, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69890713 | HCID 69890713 | — |
| Solvent | N,N-Dimethylaniline | HCID 949 | — |
| Product | HCID 86586191 | HCID 86586191 | 34.1% |
Reaction Steps
0.82 g of 5-(2-butenyloxy)-6-t-butyl-2,3-dihydrobenzofuran-2-spiro-1′-cycloheptane was dissolved in 3 ml of dimethylaniline and the solution was treated in the same manner as in Example 8-2) to give 0.14 g of 6-t-butyl-5-hydroxy-4-(1-methyl-2-propenyl)-2,3-dihydrobenzofuran-2-spiro-1′-cycloheptane as a white solid (yield 17%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06403639B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-893b244cbc5c4181a72bf21e5f955b7a |
| Source note | uspto-grants-2002_06 |