Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2186283Generated: October 30, 2026

HCID 86586191, compound → HCID 86586192, compound

https://huagongshe.com/reaction/2186283

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86586191HCID 86586191—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 86586192HCID 8658619271%

Reaction Steps

0.07 g of 6-t-butyl-5-hydroxy-4-(1-methyl-2-propenyl)-2,3-dihydrobenzofuran-2-spiro-1′-cycloheptane synthesized in Example 12 was dissolved in 10 ml of ethanol and he solution was treated with 0.01 g of 10% palladium on carbon in the same manner as in Example 9 to give 0.05 g of 6-t-butyl-5-hydroxy-4-(1-methylpropyl)-2,3-dihydrobenzofuran-2-spiro-1′-cycloheptane as a pale yellow oil (yield 71%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06403639B1
Source datasetuspto-grants-2002_06
ORD IDord-3097e79386e641e58b373630bf1987c3
Source noteuspto-grants-2002_06