Ammonia → HCID 10878919, compound

Participants

Reaction Steps

A suspension consisting of 60 g of azobisisobutyronitrile, 28 g of methanol and 270 ml of toluene was reacted by introducing 32 g of hydrogen chloride to obtain a toluene suspension of 2,2′-azobis(1-imino-1-methoxy-2-methylpropane) hydrochloride. The toluene suspension was neutralized with ammonia, followed by filtering to obtain a toluene solution of 2,2′-azobis(1-imino-1-methoxy-2-methylpropane). To the toluene solution was added 62 g of pyrrolidine, and reacted for 7 hours. After standing overnight, ethyl acetate was poured into the reaction solution, and crystals ware filtered and dried to obtain 10 g of pale yellow crystal of 2,2′-azobis [2-methyl-1-(N-pyrrolidinyl)iminopropane].

Provenance & Evidence