HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21348554, compound → HCID 21348552, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21348554 | HCID 21348554 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21348552 | HCID 21348552 | 95% |
Reaction Steps
To a solution of (S)-(+)-N-Boc-2-styrylpyrrolidine (0.56 g, 2.1 mmol) in 10 mL of methanol was added a catalytic amount of 10% Pd/C. The mixture was hydrogenated on a Parr shaker at 50 psi for 5 h. The mixture was filtered and the solution was concentrated under reduced pressure to give the title compound as a light yellow oil (0.53 g, 95%). ES (+) MS m/e=276 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06403792B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-5cc027f49f904c88a90b4a647103f6e4 |
| Source note | uspto-grants-2002_06 |