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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2186477Generated: October 31, 2026

HCID 21348554, compound → HCID 21348552, compound

https://huagongshe.com/reaction/2186477

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 21348554HCID 21348554—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 21348552HCID 2134855295%

Reaction Steps

To a solution of (S)-(+)-N-Boc-2-styrylpyrrolidine (0.56 g, 2.1 mmol) in 10 mL of methanol was added a catalytic amount of 10% Pd/C. The mixture was hydrogenated on a Parr shaker at 50 psi for 5 h. The mixture was filtered and the solution was concentrated under reduced pressure to give the title compound as a light yellow oil (0.53 g, 95%). ES (+) MS m/e=276 (M+H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06403792B1
Source datasetuspto-grants-2002_06
ORD IDord-5cc027f49f904c88a90b4a647103f6e4
Source noteuspto-grants-2002_06