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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2186539Generated: October 29, 2026

Peracetic Acid → Peracetic Acid

https://huagongshe.com/reaction/2186539

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPeracetic AcidHCID 6585—
ReactantCodeinoneHCID 5459910—
SolventDiethyl EtherHCID 3283—
ProductPeracetic AcidHCID 6585—
Product(4R,4aS,12bS)-4a-hydroxy-9-methoxy-3-methyl-2,4,7a,13-tetrahydro-1H-4,12-methanobenzofuro[3,2-e]isoquinolin-7-oneHCID 5359420—

Reaction Steps

14-Hydroxycodeinone was synthesized from the dienolsilyl ether of codeinone by oxidative hydroxylation using a peracetic acid solution preparation. The peracetic acid solution was prepared as follows:

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06403798B2
Source datasetuspto-grants-2002_06
ORD IDord-5552df700b994e2db69b7906733678d5
Source noteuspto-grants-2002_06