Methanol → HCID 59896206, compound

HRID 2186559Notes

Reaction equation

HRID 2186559 reaction equation
[NH2:1][CH2:2][CH2:3][S:4][CH2:5][C@@H:6]([C:8]([OH:10])=[O:9])[NH2:7].[CH3:11]O>>[NH2:1][CH2:2][CH2:3][S:4][CH2:5][C@@H:6]([C:8]([O:10][CH3:11])=[O:9])[NH2:7]

Participants

3

Reactant 2

HCID 887MethanolHCID 99558S-(2-Aminoethyl)-L-cysteine

Product 1

HCID 59896206HCID 59896206, compound

Procedure

A 10 g (50 mmol) sample of S-(2-aminoethyl)-L-cysteine was dissolved in 400 mL of methanol. Into this cooled solution was bubbled in anhydrous HCl for 30 minutes. After stirring at room temperature overnight, the solution was concentrated to afford 12.7 g of the title compound.

Workup

  1. customInto this cooled solution was bubbled in anhydrous HCl for 30 minutes
  2. concentrationthe solution was concentrated

Sources & evidence

ORD record
ord-1c241fbd630446c8871a2b17a413783e
Source dataset
uspto-grants-2002_06
Patent number
US06403830B2

Reaction notes

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