HCID 22448989, compound → HCID 21349911, compound

HRID 2186745Notes

Reaction equation

HRID 2186745 reaction equation
O[CH2:2][CH2:3][N:4]1[C:9]2[CH:10]=[CH:11][CH:12]=[C:13]([O:14][CH2:15][C:16]([O:18][CH3:19])=[O:17])[C:8]=2[O:7][CH2:6][CH2:5]1.[C:20]1([C:26]([C:30]2[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=2)([CH3:29])[CH2:27][SH:28])[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1>>[C:30]1([C:26]([C:20]2[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=2)([CH3:29])[CH2:27][S:28][CH2:2][CH2:3][N:4]2[C:9]3[CH:10]=[CH:11][CH:12]=[C:13]([O:14][CH2:15][C:16]([O:18][CH3:19])=[O:17])[C:8]=3[O:7][CH2:6][CH2:5]2)[CH:31]=[CH:32][CH:33]=[CH:34][CH:35]=1

Participants

3

Reactant 2

HCID 22448989HCID 22448989, compoundHCID 23086889HCID 23086889, compound

Product 1

HCID 21349911HCID 21349911, compoundYield 37.5%

Procedure

The same process as Example 1 was repeated except that methyl (4-(2-hydroxyethyl)-3,4-dihydro-2H-1,4-benzoxazin-8-yloxy)acetate (200 mg) and 2,2-diphenylpropanethiol (410 mg) were used to obtain the colorless oily object compound (134 mg, yield 37%).

Sources & evidence

ORD record
ord-3a28b561abda47d4a458892ecb6b9a9a
Source dataset
uspto-grants-2002_06
Patent number
US06407096B1

Reaction notes

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