Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | HCID 70156897 | HCID 70156897 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 22449479 | HCID 22449479 | — |
Reaction Steps
1.29 gm of the compound prepared in (1) above was dissolved into 30 ml of acetic acid. After the addition of 339 mg of hydroxylamine hydrochloride, the mixture was heated for 10 minutes at 120° C. while stirring. After cooling, water was added to collect the precipitate by filtration. The precipitate was washed with water and hexane to obtain 1.1 gm of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06407115B1 |
|---|
| Source dataset | uspto-grants-2002_06 |
|---|
| ORD ID | ord-0e7ee1e6619c4a8eb4b77f0772630ec5 |
|---|
| Source note | uspto-grants-2002_06 |
|---|
