2,8-Diacetylamino-1-tetralone → HCID 22449464, compound

HRID 2186847Notes

Reaction equation

HRID 2186847 reaction equation
C(C1CCC2C(=C(C(=O)C)C=CC=2[C:14]#[N:15])C1=O)(=O)C.[C:20]([NH:23][CH:24]1[CH2:33][CH2:32][C:31]2[C:26](=[C:27]([NH:34]C(=O)C)[CH:28]=[CH:29][CH:30]=2)[C:25]1=[O:38])(=[O:22])[CH3:21]>>[C:20]([NH:23][CH:24]1[CH2:33][CH2:32][C:31]2[C:26](=[C:27]([NH2:34])[CH:28]=[CH:29][C:30]=2[C:14]#[N:15])[C:25]1=[O:38])(=[O:22])[CH3:21]

Participants

3

Reactant 2

HCID 120472982,8-Diacetylamino-1-tetraloneHCID 22449413HCID 22449413, compound

Product 1

HCID 22449464HCID 22449464, compound

Procedure

The reaction was carried out in the same manner as in Example 1-(4), except that 250 mg of the compound prepared in (1) above was used instead of 2,8-diacetylamino-1-tetralone of Example 1-(4), and post-treated to produce 182 mg of the title compound.

Workup

  1. additionpost-treated

Sources & evidence

ORD record
ord-1eaa1e1ed1f648188c77f1611963f83f
Source dataset
uspto-grants-2002_06
Patent number
US06407115B1

Reaction notes

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