2,8-Diacetylamino-1-tetralone → HCID 22449520, compound

HRID 2186853Notes

Reaction equation

HRID 2186853 reaction equation
[C:1]([NH:4][CH:5]1[CH2:14][CH2:13][C:12]2[C:7](=[C:8]([NH:19]C(=O)C)[CH:9]=[CH:10][C:11]=2[NH:15]C(=O)C)[C:6]1=[O:23])(=[O:3])[CH3:2].C(NC1CCC2C(=C(NC(=O)C)C=CC=2)C1=O)(=O)C>>[C:1]([NH:4][CH:5]1[CH2:14][CH2:13][C:12]2[C:7](=[C:8]([NH2:19])[CH:9]=[CH:10][C:11]=2[NH2:15])[C:6]1=[O:23])(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 120472982,8-Diacetylamino-1-tetraloneHCID 23184196HCID 23184196, compound

Product 1

HCID 22449520HCID 22449520, compound

Procedure

The reaction was carried out in the same manner as in Example 1-(4), except that 500 mg of the compound prepared in (1) above was used instead of 2,8-diacetylamino-1-tetralone of Example 1-(4), and post-treated to produce 290 mg of the title compound.

Workup

  1. additionpost-treated

Sources & evidence

ORD record
ord-b99cb157d3fc437482df5deac1325b46
Source dataset
uspto-grants-2002_06
Patent number
US06407115B1

Reaction notes

Loading…