HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 6938234, compound → HCID 67184367, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 6938234 | HCID 6938234 | — |
| Reactant | 5-Benzyloxy-1,2,3,4-tetrahydronaphthalene-1-carboxylic acid | HCID 11208318 | — |
| Product | HCID 67184367 | HCID 67184367 | 80.8% |
Reaction Steps
By the reaction and treatment in the same manner as in Example 12 using 5-benzyloxy-1,2,3,4-tetrahydronaphthalene-1-carboxylic acid (0.57 g) and [(4-dimethylaminophenyl)methyl]phenylamine (0.61 g) as starting materials, 5-benzyloxy-N-[(4-dimethylaminophenyl)methyl]-N-phenyl-1,2,3,4-tetrahydronaphthalene-1-carboxamide (0.80 g) was obtained. By the reaction and treatment in the same manner as in Example 17 using this compound, N-[(4-dimethylaminophenyl)methyl]-5-hydroxy-N-phenyl-1,2,3,4-tetrahydronaphthalene-1-carboxamide (0.083 g) was obtained. melting point: 138-143° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08198454B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-e6dea13d5e2b49f4a4ac508496f8b6f9 |
| Source note | uspto-grants-2012_06 |