HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 2-Methylprop-2-enoic acid--butyl prop-2-enoate (1/1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Acrylic Acid | HCID 6581 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methylene-bisacrylamide | HCID 53800990 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2-Methylprop-2-enoic acid--butyl prop-2-enoate (1/1) | HCID 159986 | — |
Reaction Steps
An aqueous monomer phase was formed containing 40 g acrylic acid, 36.2 g of 46% sodium hydroxide solution, 0.03 g methylenebisacrylamide and 73.8 g water. A continuous phase was formed of 500 g ethyl acetate and 20 g of a stabiliser of composition butyl acrylate/methacrylic acid (90/10 by weight), prepared in a similar manner to Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06407161B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-5529e31655864cd49f47469b71125515 |
| Source note | uspto-grants-2002_06 |