HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-5-(chloromethyl)pyridine → N-((2-Chlorothiazol-5-yl)methyl)ethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-5-(chloromethyl)pyridine | HCID 155479 | — |
| Reactant | 2-Chloro-5-chloromethylthiazole | HCID 2763179 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-((2-Chlorothiazol-5-yl)methyl)ethanamine | HCID 22450338 | — |
Reaction Steps
The reaction procedure of Reference Example 17 was repeated except that crude 2-chloro-5-chloromethylthiazole was used in lieu of 6-chloro-3-pyridylmethyl chloride and that CH2Cl2 was used as the extractant. The procedure gave the title compound as a crude oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06407248B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-66d33d5db1814895aa70aabb5053102c |
| Source note | uspto-grants-2002_06 |