HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl aluminum cyanide → HCID 57026814, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl aluminum cyanide | HCID 16686413 | — |
| Reactant | HCID 57222965 | HCID 57222965 | — |
| Product | HCID 57026814 | HCID 57026814 | — |
Reaction Steps
1.54 g ergosta-4,8,22-trien-3-one were treated with 11.73 ml diethylaluminum cyanide solution (1 N, toluene) as described in example 58. After aqueous work up and chromatography 0.90 g 5-cyano-5α-ergosta-8,22-dien-3-one were isolated as a white solid (beside the corresponding 5β-cyano-compound).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06407086B2 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-a0e29a25cc4a47d8afab6ce5d614f314 |
| Source note | uspto-grants-2002_06 |