HuagongsheHuagongshe Chemistry Print Report · For research reference only
Silane, chloro(chloromethyl)dimethyl- → n-Ethyl-2-chloro-6-[(chloromethyl)dimethylsilyl]benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Silane, chloro(chloromethyl)dimethyl- | HCID 74393 | — |
| Reactant | 2-chloro-N-ethylbenzamide | HCID 347962 | — |
| Product | n-Ethyl-2-chloro-6-[(chloromethyl)dimethylsilyl]benzamide | HCID 18630074 | — |
Reaction Steps
The title compound was prepared from the compound of Example f and 2.0 eq (chloromethyl)dimethylsilyl chloride according to General Method C. Recrystallization from ethyl acetate gave 3.0 g of the desired compound as a white solid, a 52% yield. m.p. 88-89° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06410558B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-e30350ef93ea4a55bb23f820585da39d |
| Source note | uspto-grants-2002_06 |