3,4-Dichlorophenol → HCID 12017031, compound

HRID 2188262Notes

Reaction equation

HRID 2188262 reaction equation
[Br:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[O:7])=[C:4](F)[CH:3]=1.[Cl:11][C:12]1[CH:13]=[C:14]([OH:19])[CH:15]=[CH:16][C:17]=1[Cl:18]>>[Br:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[O:7])=[C:4]([O:19][C:14]2[CH:15]=[CH:16][C:17]([Cl:18])=[C:12]([Cl:11])[CH:13]=2)[CH:3]=1

Participants

3

Reactant 2

HCID 72583,4-DichlorophenolHCID 1435174-Bromo-2-fluorobenzaldehyde

Product 1

HCID 12017031HCID 12017031, compoundYield 46.9%

Procedure

In the same manner, reaction of 12.06 g of 4-bromo-2-fluorobenzaldehyde and 9.68 g of 3,4-dichlorophenol gave 9.64 g of 4-bromo-2-(3,4-dichlorophenoxy)-benzaldehyde as pale yellow crystals.

Sources & evidence

ORD record
ord-a23123ca8a56470c973e56bb30a32059
Source dataset
uspto-grants-2002_06
Patent number
US06410736B1

Reaction notes

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