HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Acetoxyisobutyroyl chloride → HCID 86598622, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Acetoxyisobutyroyl chloride | HCID 123496 | — |
| Reactant | HCID 67401517 | HCID 67401517 | — |
| Product | HCID 86598622 | HCID 86598622 | 98% |
Reaction Steps
A solution of 1-chlorocarbonyl-1-methylethyl acetate (10 mmol) and (E)-2,4,6-trimethoxystyryl-3-amino-4-methoxybenzylsulfone (10 mmol) was reacted according to General Method A. The crude product obtained was purified by column chromatography to yield the desired product in 98% yield. (m.p. 148-150° C.)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08324190B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-360bcb351baa48b3b21a9a14aae4ee7f |
| Source note | uspto-grants-2012_12 |