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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2188874Generated: October 30, 2026

p,p'-Dimethoxybenzhydryl alcohol → 4-(4,4'-Dimethoxybenzhydryl)-thiophenyl boronic acid

https://huagongshe.com/reaction/2188874

Reaction equation

Participants

RoleNameHCIDCharge
Reactantp,p'-Dimethoxybenzhydryl alcoholHCID 69768—
Reactant4-Mercaptophenylboronic acidHCID 4431894—
SolventAcetic AcidHCID 176—
Product4-(4,4'-Dimethoxybenzhydryl)-thiophenyl boronic acidHCID 67120687—

Reaction Conditions

Temperature60 °C

Reaction Steps

4,4′-Dimethoxybenzhydrol (2.7 g, 11 mmol) and 4-mercaptophenylboronic acid (1.54 g, 10 mmol) were dissolved in 20 mL AcOH and heated at 60° C. for 1 h. Solvent was evaporated and the residue was dried under high vacuum. This material was used without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08324207B2
Source datasetuspto-grants-2012_12
ORD IDord-f9e83b7a9cee4ab3bac63a284a031f15
Source noteuspto-grants-2012_12