HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Acetate → 2-Chloro-3-(2-fluoro-4-iodo-phenylamino)-isonicotinamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Reactant | 2-Chloro-3-(2-fluoro-4-iodophenylamino)-isonicotinic acid | HCID 57649634 | — |
| Product | 2-Chloro-3-(2-fluoro-4-iodo-phenylamino)-isonicotinamide | HCID 11668292 | — |
Reaction Steps
2-Chloro-3-(2-fluoro-4-iodo-phenylamino)-isonicotinamide was synthesized according to the procedure for General Method 1, outlined above, starting with 0.2 mmol of 2-Chloro-3-(2-fluoro-4-iodo-phenylamino)-isonicotinic acid and 0.5 mmol of ammonium acetate. LC/MS [8.61 min; 392 (M+1)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08198457B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-f151c05959054482ace63f043b9baadd |
| Source note | uspto-grants-2012_06 |