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HRID218922

反应详情

EQUATION

反应方程式

HRID 218922 的结构方程式

REACTANTS

反应物

2
结构：ClCCl.O=C(O)C(F)(F)F
HCID21863450

未命名化合物

结构：CC(C)(C)OC(=O)NNC(=O)c1ccncc1Nc1ccc(I)cc1F
HCID57649630

未命名化合物

PRODUCTS

生成物

1
结构：Cl.NNC(=O)c1ccncc1Nc1ccc(I)cc1F
HCID67249879

未命名化合物

PROCEDURE

实验过程

3-[(2-fluoro-4-iodophenyl)amino]isonicotinohydrazide hydrochloride was synthesized from tert-butyl 2-{3-[(2-fluoro-4-iodophenyl)amino]isonicotinoyl}hydrazine-carboxylate (described earlier) by deprotection of the Boc group under acidic conditions (50:50 TFA/DCM). LC/MS [7.11 min; 373 (free base, M+1)]

WORKUP

后处理

  1. customLC/MS [7.11 min; 373 (free base, M+1)]